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Effects of Reflow Profile and Thermal Conditioning on Intermetallic Compound Thickness for SnAgCu Soldered Joints

机译:回流曲线和热条件对SnAgCu焊接接头金属间化合物厚度的影响

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摘要

Purpose – The purpose of this paper is to investigate the effects of reflow time, reflow peak temperature, thermal shock and thermal aging on the intermetallic compound (IMC) thickness for Sn3.0Ag0.5Cu (SAC305) soldered joints. Design/methodology/approach – A four-factor factorial design with three replications is selected in the experiment. The input variables are the peak temperature, the duration of time above solder liquidus temperature (TAL), solder alloy and thermal shock. The peak temperature has three levels, 12, 22 and 32°C above solder liquidus temperatures (or 230, 240 and 250°C for SAC305 and 195, 205, and 215°C for SnPb). The TAL has two levels, 30 and 90 s. The thermally shocked test vehicles are subjected to air-to-air thermal shock conditioning from -40 to 125°C with 30 min dwell times (or 1 h/cycle) for 500 cycles. Samples both from the initial time zero and after thermal shock are cross-sectioned. The IMC thickness is measured using scanning electron microscopy. Statistical analyses are conducted to compare the difference in IMC thickness growth between SAC305 solder joints and SnPb solder joints, and the difference in IMC thickness growth between after thermal shock and after thermal aging. Findings – The IMC thickness increases with higher reflow peak temperature and longer time above liquidus. The IMC layer of SAC305 soldered joints is statistically significantly thicker than that of SnPb soldered joints when reflowed at comparable peak temperatures above liquidus and the same time above liquidus. Thermal conditioning leads to a smoother and thicker IMC layer. Thermal shock contributes to IMC growth merely through high-temperature conditioning. The IMC thickness increases in SAC305 soldered joints after thermal shock or thermal aging are generally in agreement with prediction models such as that proposed by Hwang. Research limitations/implications – It is still unknown which thickness of IMC layer could result in damage to the solder. Practical implications – The IMC thickness of all samples is below 3 µm for both SnPb and SAC305 solder joints reflowed at the peak temperature ranging from 12 to 32°C above liquidus temperature and at times above liquidus ranging from 30 to 90 s. The IMC thickness is below 4 µm after subjecting to air-to-air thermal shock from -40 to 125°C with 30 min dwell time for 500 cycles or thermal aging at 125°C for 250 h. Originality/value – The paper reports experimental results of IMC thickness at different thermal conditions. The application is useful for understanding the thickness growth of the IMC layer at various thermal conditions.
机译:目的–本文的目的是研究回流时间,回流峰值温度,热冲击和热老化对Sn3.0Ag0.5Cu(SAC305)焊接接头的金属间化合物(IMC)厚度的影响。设计/方法/方法–在实验中选择了具有三个重复的四因子析因设计。输入变量是峰值温度,高于焊料液相线温度(TAL)的持续时间,焊料合金和热冲击。峰值温度比焊料液相线温度高12、22和32°C(对于SAC305为230、240和250°C,对于SnPb为195、205和215°C)三个水平。 TAL有两个级别,分别为30和90 s。热冲击试验车辆在-40至125°C的温度下进行空对空热冲击调节,保压时间为30分钟(或1小时/循环),持续500个循环。从初始时间零和热冲击之后的样品均被横切。使用扫描电子显微镜测量IMC厚度。进行统计分析以比较SAC305焊点和SnPb焊点之间的IMC厚度增长的差异,以及热冲击后和热老化后的IMC厚度增长的差异。发现– IMC厚度随着回流峰值温度的升高和液相线以上时间的延长而增加。当在高于液相线和高于液相线的相同峰值温度下回流时,SAC305焊点的IMC层在统计上比SnPb焊点的IMC层厚得多。热调节会导致更平滑,更厚的IMC层。热冲击仅通过高温调节就有助于IMC的增长。热冲击或热老化后,SAC305焊点中的IMC厚度增加通常与Hwang提出的预测模型一致。研究的局限性/意义–仍然不清楚哪种IMC层厚度会导致焊料损坏。实际意义–对于锡铅和SAC305焊点,在高于液相线温度12至32°C的峰值温度和高于液相线30至90 s的时间回流的所有样品的IMC厚度均低于3 µm。在-40至125°C的空气-空气热冲击下,经过30分钟的停留时间进行500次循环或在125°C的温度下进行250小时的热老化之后,IMC的厚度低于4 µm。原创性/价值–本文报告了在不同热条件下IMC厚度的实验结果。该应用对于理解各种热条件下IMC层的厚度增长很有用。

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